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Houben-Weyl Methods in Organic Chemistry: Carboxylic Acid, by Houben J., Weyl T.

By Houben J., Weyl T.

Methoden der Organischen Chemie (Methods of natural Chemistry, known as Houben-Weyl) is a typical reference paintings for chemists engaged in natural synthesis. In volumes on compound periods, together with all Supplemental volumes, preparative equipment are taken care of comprehensively and severely. Tables of examples evaluate crucial tools and convey their scope. special experimental methods are given for the simplest equipment. The reactivity and extra reactions of every compound classification also are offered. The huge use of formulation schemes assist in making the German-language volumes extra without difficulty comprehensible to non-German readers.

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Fm Seite 52 Dienstag, 25. A. Davis · K. Matyjaszewski synthesis was reversed and pSt macroinitiators were used for nBMA polymerization, the results were similar. Again, the molecular weight distributions broadened after chain extensions [184]. Ying et al. prepared block copolymers of both MMA and HEMA with St [186]. 28, respectively [186]. 28) was chain extended with St, the macroinitiator was consumed slowly at 110 °C, as evidenced by the presence of a low molecular weight shoulder in the GPC traces that persisted until >40% monomer conversion.

Fm Seite 35 Dienstag, 25. Juni 2002 9:45 09 3 Linear Block Copolymers 35 pared containing an a-carboxy functionality was used successfully to prepare the functional copolymers, which were proposed for different types of postfunctionalization reactions [101]. Armes et al. prepared TEMPO-capped poly(sodium 4-styrenesulfonate) (SSt) using potassium persulfate as the initiator in refluxing solution of a 3:1 v:v mixture of ethylene glycol and water at 120 °C [150], which was then used as a macroinitiator for the successful preparation of block copolymers with 4-(dimethylamino)methylstyrene (DMAMS) and sodium 4-styrenecarboxylate (SSC).

186] Ying et al. [186] Ying et al. [186] Pan et al. [187] Schubert et al. [188] Qiu et al. fm Seite 55 Dienstag, 25.

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