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Organic Chemistry

Advanced organic synthesis: methods and techniques by Richard S. Monson

By Richard S. Monson

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Extra resources for Advanced organic synthesis: methods and techniques

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Tarbell, /. Org. Chem. 33, 3797 (1968). G. A. Wiley, R. L. Hershkowitz, B. M. Rein, and B. C. Chung, /. Amer. Chem. Soc. 86,964 (1964). D. Levy and R. Stevenson, J. Org. Chem. 30, 3469 (1965). J. P. Schaefer, J. G. Higgins, and P. K. Shenov, Org. Syn. 48, 51 (1968). REFERENCES 53 7. C. Djerassi, Chem. Rev. 43, 271 (1948); L. Horner and E. H. Winkelmann in "Newer Methods of Preparative Organic Chemistry" ( W. ), Vol. 3, Academic Press, New York, 1964. 8. N. S. Isaacs, "Experiments in Physical Organic Chemistry," p.

Rev. 12, 17 (1958). 2. R. A. Benkeser and E. M. Kaiser, /. Org. Chem. 29, 955 (1964). 3. L. Reggel, R. A. Friedel, and I. Wender,/. Org. Chem. 22, 891 (1957); W. G. Dauben, E. C. Martin, and G. J. Fonken, J. Org. Chem. 23, 1205 (1958). 4. G. Stork and S. D. Darling, /. Amer. Chem. Soc. 86, 1761 (1964) and references cited therein. 5. E. E. van Tamelen and W. C. Proost, J. Amer. Chem. Soc. 76, 3632 (1954). 6. M. Yanagita, K. Yamakawa, A. Tahara, and H. Ogura, /. Org. Chem. 20, 1767 (1955). 7. P.

Tamm, and P. E. Aldrich, /. Amer. Chem. Soc. 91, 7315 (1969). 9. W. Huckel and W. Kraus, Chem. Ber. 92, 1158 (1959). Hydroboration A remarkable variation of the hydride reduction is the addition to double bonds of diborane (B2H6) (7). Easily generated by the reaction of boron trifluoride etherate with sodium borohydride, the reagent may be used in the generating solution or may be distilled into a receiving flask containing an ether as solvent. Diborane reacts with unsaturated polar functional groups with results similar to those of the metal hydride reducing agents.

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