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Advanced ESR Methods in Polymer Research by Shulamith Schlick

By Shulamith Schlick

A definitive paintings on ESR and polymer technology by way of modern day major authoritiesThe earlier two decades have visible outstanding advances in electron spin resonance (ESR) innovations, really as they observe to polymeric fabrics. With contributions from over a dozen of the world's most sensible polymer scientists, complex ESR equipment in Polymer examine is the 1st booklet to compile the entire present tendencies during this interesting box into one entire reference.Part I establishes the basics of ESR, from experimental innovations to facts research, and serves as a invaluable evaluation for the start ESR scholar. half II introduces the large variety of ESR functions to polymeric structures, together with dwelling radical polymerization, block copoly-mers, polymer recommendations, ion-containing polymers, polymer lattices, membranes in gas cells, degradation, polymer coatings, dendrimers, and conductive polymers. via exposing readers to the good power of ESR, the authors desire to motivate extra vast program of those tools.

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Advanced ESR Methods in Polymer Research

A definitive paintings on ESR and polymer technology by way of latest prime authoritiesThe previous two decades have visible striking advances in electron spin resonance (ESR) options, relatively as they follow to polymeric fabrics. With contributions from over a dozen of the world's best polymer scientists, complicated ESR tools in Polymer examine is the 1st e-book to compile the entire present traits during this fascinating box into one entire reference.

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22. Plots of log(Ϫlog(D(t)) versus log(t) exhibit a linear dependence with slope of x/3. qxd 38 8/4/2006 7:36 PM Page 38 DOUBLE RESONANCE ESR METHODS concentration suggested that the first component corresponds to counterions in the vicinity of an isolated and locally stretched chain, while the second component corresponds to counterions in regions where chains overlap. 4. Direct Computation of Distance Distributions The primary result of a pulsed ELDOR measurement is a distribution of dipolar couplings d.

5 for the enrichment or depletion of ionic spin probes close to a charged surface. By using the analytical solution of the Poisson–Boltzmann equation for a charged planar plate in an electrolyte solution,19 we have calculated the concentration profiles of monovalent ions in solution with the opposite (Fig. 5a) or the same (Fig. 5c) charge as the platelet. Assuming that the observer spins S are attached to the surface of the platelet and the pumped spins are located at the ions in solution, we obtain the dipolar evolution functions B(t) shown as solid lines in Fig.

18. ; Academic Press: New York, 1979. 19. Biological Magnetic Resonance. ; Plenum: New York, 1989; Vol 8. 20. ; Schlick, S. In Instrumental Methods in Electron Magnetic Resonance, Biological Magnetic Resonance, Vol. ; Kluwer Academic/Plenum Publishing Corporation: New York, 2004; pp. 349–384. 21. , Eds. Symposium Series Vol. 1; MMI Press: Harwood, Chur, 1980. 22. G. : Chichester, UK, 1996; Chapt. 9, pp. 231–252. 23. ; Huber, W. Electron Spin Resonance Spectroscopy of Organic Radicals, WileyVCH: Weinheim, 2003.

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